Loading...
The URL can be used to link to this page
Your browser does not support the video tag.
WQ Subcommittee Backup Documents 10/01/2019
C SG rali ) .�� 4..v^. oUwt. 14A-Y-V." (- Colyer County TM POLLUTION CONTROL LIVE GREEN. SAVE BLUE. www. LiveGreenSaveBlue.com Report To: Tonia Selmeski City of Marco Island 50 Bald Eagle Drive Marco Island.FL 34145 Collected by: CCPCD Collection Date: 08/07/2019 Submittal Date: 08/07/2019 'a' 12:34 Report Date: 9/5/2019 Report Time: 10:31:32AM Project: MARCO Report#: 0819_M RCO_1 Data Qualifier Code Key: I: The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit U: The compound was analyzed for but not detected Q: Sample held beyond acceptable holding time 1: Estimate value:the reported value failed to meet established criteria for either precision or accuracy V: Analyte detected in both the sample and the associated method blank B: Colony count is generated from plates in which the total number of colonies is outside the method indicated ideal range Y: The laboratory analysis was from an improperly preserved sample.The data may not be accurate. G: Indicates that the analyte was detected at or above the method detection limit in both the sample and the associated field blank.equipment blank.or trip blank-and the blank value was greater than 10%of the associated sample value. Analyses performed using EPA or Standard Methods and certified to meet NELAC Standards.Data qualifiers assigned according to F.A.C.62-160. Results contained in this report relate only to the samples collected. Respectfully Submitted, x", '13 NosbaPeer4, tik* j Nosbel Perez • _ B'' r Laboratory Supervisor ANALYTICAL RESULTS Report#0819_MRCO_I Location: WINDMILL Field ID: AF56187 Lab ID: AF56187 Collect Date/Time: 817119 08:56 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N <MDL U me/L 0.011 0.020 1 08109/2019 12:08 Enterococci Enterolert/QT 10 <130 U MPN/100 mL 10 10 10 08/07/2019 14.22 Digestion for Metals EPA 200.8 Completed 7 08/13/2019 09:25 Phosphorus-Total EPA 200.8 0.084 <0.046 mg/L 0.028 0.070 7 08/15/2019 12:09 Nitrogen-Total Kjeldahl EPA 351.2 0.665 mg/L 0.230 0.500 1 08/19/2019 16:02 Nitrate-Nitrite(N) EPA 353.2 0.011 U mg/L 0.011 0.020 1 08/08/2019 14:09 pH FDEP FTI 100 7.8 6.5-8.5 SU I 08/07/2019 08:56 Dissolved Oxygen Saturation FDEP FT1500 74.1 >42 % I 08/07/2019 08:56 Nitrogen-Total Nitrogen-Total 0.665 <0.3 mg/L 0.230 0.500 1 08/20/2019 09:26 Chlorophyll a SM 10200 H 6.8 <4.9 mg/m3 1.00 1.00 1 08/23/2019 13:02 Filtration for Chlorophyll and Pht SM 10200 H Completed I 08/07/2019 14:31 Pheophytin SM 10200 H 3.50 mg/m3 1.00 1.00 I 08/23/2019 13:02 Digestion for TKN SM 4500 NorgD Complete 1 08/14/2019 13:15 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 I 08/08/2019 15:41 ANALYTICAL RESULTS Report#0819_MRCO_I Location: HOLLYHOCK Field ID: AF56188 Lab ID: AF56188 Collect Date/Time: 8/7/19 09:19 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N 0.016 I mg/L 0.011 0.020 I 08/09/2019 12:08 Enterococci Enterolert/QT 10 <130 U MPN/100 mL 10 10 10 08/07/2019 14:22 Digestion for Metals EPA 200.8 Completed 7 08/132019 09:25 Phosphorus-Total EPA 200.8 0.072 <0 046 me/L 0.028 0.070 7 08/15/2019 12:19 Nitrogen-Total Kjeldahl EPA 351.2 0.911 mg/L 0.230 0.500 1 08/19/2019 17:38 Nitrate-Nitrite(N) EPA 353.2 0.016 I mg/L 0.011 0.020 1 08/08/2019 14:15 pH FDEP FTI 100 7.7 65-8.5 SU 1 08/07/2019 09:19 Dissolved Oxygen Saturation FDEP FTI500 77.8 >42 % I 08/07/2019 09:19 Nitrogen-Total Nitrogen-Total 0.927 <0.3 mg/L 0.230 0.500 I 08/20/2019 09:26 Chlorophyll a SM 10200 H 6.0 <4.9 1 mglm3 100 1.00 I 08/23/2019 13:02 Filtration for Chlorophyll and Phe SM 10200 H Completed 1 08/07/2019 14:31 Pheophytin SM 10200 H 1.00 U1 mg/m3 1.00 1.00 1 08/23/2019 13:02 Digestion for TKN SM 4500 NorgD Complete 1 08/14/2019 13:15 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 I 08/08/2019 15:45 ANALYTICAL RESULTS Report#0819_MRCO 1 Location: HUMMINGBIRD Field ID: AF56189 Lab ID: AF56189 Collect Datelime: 817/19_ 09:46 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time _ CC-Nitrate-N CC-Nitrate-N <MDL U mg/L 0.011 0.020 1 08/09/2019 12:08 Enterococci Enterolert/QT 10 <130 MPN/100 mL 10 10 10 08/072019 14:22 FL State Laboratory ID:E45464 EPA Lab Code:F100919 Page 2 of 8 Digestion for Metals EPA 200.8 Completed 7 08/13/2019 09:25 Phosphorus-Total EPA 200.8 0.077 <0.046 mg/1 0.028 0.070 7 08/15/2019 12:22 Nitrogen-Total Kjeldahl EPA 351.2 0.684 me/L 0 230 0.500 I 08/15/2019 I I:5€ Nitrate-Nitrite(N) ERA 353.2 0.011 U malL 0.011 0.020 I 08/08/2019 14:17 pH FDEP FTI 100 7.7 6.5-8.5 SU I 08/07/2019 09:46 Dissolved Oxygen Saturation FDEP FTI500 86.2 >42 % I 08/07/2019 09:46 Nitrogen-Total Nitrogen-Total 0.684 <0.3 mg/L 0.230 0.500 1 08/15/2019 1529 Chlorophyll a SM 10200 H 8.4 <4.9 mg/m3 1.00 1.00 1 08/23/2019 13:02 Filtration for Chlorophyll and Phc SM 10200 H Completed 1 08/08/2019 11.30 Pheophytin SM 10200 H 1.00 U mg/m3 1.00 1.00 I 08/23/2019 13:02 Digestion for TKN SM 4500 NorgD Complete I 08/13/2019 09:54 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 1 08/08/2019 15:46 ANALYTICAL RESULTS Report 4 0819_MRCO_I Location: MCILVAINE Field ID: AF56190 Lab ID: AF56190 Collect Date/Time: 817/19 10:26 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N <MDL U mg/L 0.011 0.020 I 08/09/2019 12:08 Enterococci Enterolert/QT 10 <130 MPN/100 mL 10 10 10 08/07/2019 14:22 Digestion for Metals EPA 200.8 Completed 8 08/13/2019 09:25 Phosphorus-Total EPA 200.8 0.050 <0.046 1 mg/L 0.032 0.080 8 08/15/2019 13:07 Nitrogen-Total Kjeldahl EPA 351.2 0.704 mg/L 0.230 0500 1 08/15/2019 11:59 Nitrate-Nitrite(N) EPA 353.2 0.011 U mg/L 0.011 0.020 1 08/08/2019 14:19 pH FDEP FTI 100 8.0 6.5-8.5 SU I 08/07/2019 10:26 Dissolved Oxygen Saturation FDEP FT 1500 1002 >42 % I 08/07/2019 10.26 Nitrogen-Total Nitrogen-Total 0.704 <0.3 mg/L 0.230 0.500 1 08/15/2019 15:29 Chlorophyll a SM 10200 H 3.2 <4.9 melm3 1.00 1.00 1 08/23/2019 13:02 Filtration for Chlorophyll and Ph( SM 10200 H Completed I 08/08/2019 11:30 Pheophytin SM 10200 H 1.00 U mg/m3 1.00 1.00 I 08/23/2019 13:02 Digestion for TKN SM 4500 NorgD Complete 1 08/I3/2019 09:54 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 1 08/08/2019 15:47 ANALYTICAL RESULTS Report 4 0819_MRCO_I Location: E_%VINTERBERRY_BRIDGE Field ID: AF56191 Lab ID: AF56191 Collect DaterTinte: 8/7/19 10:50 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N <MDL U mg/L 0.011 0.020 1 08/09/2019 12:08 Enterococci Enterolert/QT 20 <130 MPN/100 mL 10 10 10 08/07/2019 14:22 Digestion for Metals EPA 200.8 Completed 8 08/13/2019 09:25 Phosphorus-Total EPA 200.8 0.056 <0.046 I mg/I_ 0.032 0 080 8 08/15/2019 13:10 Nitrogen-Total Kjeldahl EPA 351.2 0.658 mg/L 0.230 0.500 I 08/15/2019 12:03 Nitrate-Nitrite(N) EPA 353.2 0.011 U mg/L 0.011 0.020 1 08/08/2019 14:20 FL State Laboratory ID:E45464 EPA Lab Code:FL00919 Page 3 of 8 pH FDEP FTI 100 7.9 6.5-8.5 SU I 08/07/2019 10:50 Dissolved Oxygen Saturation FDEP FTI 500 98.4 >42 % 1 08/07/2019 10.50 Nitrogen-Total Nitrogen-Total 0.658 <0.3 mg/L 0.230 0.500 1 08/15/2019 1529 Chlorophyll a SM 10200 H 5.3 <4.9 mg/m3 1.00 1.00 I 08/23/2019 13:02 Filtration for Chlorophyll and Phe SM 10200 H Completed 1 08/08/2019 11:30 Pheophytin SM 10200 H 120 mg/m3 1.00 1.00 I 08/23/2019 1302 Digestion for TKN SM 4500 NorgD Complete I 08/13/2019 09:54 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 I 08/08/2019 15148 ANALYTICAL RESULTS Report#08I9_MRCO_1 Location: W_WINTERBERRY_BRIDGE Field ID: AF56192 Lab ID: AF56192 Collect Date/Time: 8/7/19 11:12 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N <MDL U mg/L 0.011 0.020 1 08/09/2019 12:08 Enterococci Enterolert/QT 10 <130 U MPN/100 mL 10 10 10 08/072019 14:22 Digestion for Metals EPA 200.8 Completed 7 08/13/2019 09:25 Phosphorus-Total EPA 200.8 0.070 . <0.046 I mg/L 0.028 0.070 7 08/15/2019 1225 Nitrogen-Total Kjeldahl EPA 351.2 0 668 mg/1. 0.230 0.500 I 08/15/2019 1202 Nitrate-Nitrite(N) EPA 3532 0.011 U mg/L 0.011 0.020 1 08/08/2019 14.22 pH FDEP FTI 100 8.0 6.5-8.5 SU I 08/07/2019 11:12 Dissolved Oxygen Saturation FDEP FT1500 108 >42 % I 08/07/2019 11:12 Nitrogen-Total Nitrogen-Total 0.668 <0.3 mg/L 0.230 0.500 1 08/15/2019 15:29 Chlorophyll a SM 10200 H 6.4 <4.9 mg/m3 1.00 1.00 I 08/232019 13:02 Filtration for Chlorophyll and Phe SM 10200 H Completed I 08/082019 11:30 Pheophytin SM 10200 H 1.00 U mg/m3 1.00 1.00 1 08/23/2019 13:02 Digestion for TKN SM 4500 NorgD Complete 1 08/13/2019 09:54 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 I 08/08/2019 15:49 ANALYTICAL RESULTS Report# 0819_MRCO_II Location: BARFIELD_BRIDGE Field ID: AF56193 Lab ID: AF56193 Collect Date/Time: 8/7/19 09:38 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N <MDL U mg/L 0.011 0.020 1 08/09/2019 12:08 Enterococci Enterolert/QT 10 <130 MPN/100 mL 10 10 10 08/07/2019 14:22 Digestion for Metals EPA 200.8 Completed 7 08/13/2019 09:25 Phosphorus-Total EPA 200 8 0.062 <0046 1 mg/L 0.028 0.070 7 08/15/2019 12:28 Nitrogen-Total Kjeldahl EPA 351 2 0.680 me/L 0.230 0.500 1 08/19/2019 16:09 Nitrate-Nitrite(N) EPA 353.2 0.011 U mg/L 0.011 0.020 I 08/082019 14:24 pH FDEP FTI 100 7.9 6.5-8.5 SU 1 08/07/2019 09:38 Dissolved Oxygen Saturation FDEP FT1500 95.2 >42 % I 08/072019 0938 Nitrogen-Total Nitrogen-Total 0.680 <0.3 mg/L 0.230 0.500 1 08/20/2019 0926 Chlorophyll a SM 10200 H 3.3 <4.9 mg/m3 1.00 1.00 I 08/23/2019 13:02 FL State Laboratory ID:E4S464 EPA Lab Code:FL00919 Page 4 of 8 Filtration for Chlorophyll and Phe SM 10200 H Completed 1 08/07/2019 14:31 Pheophytin SM 10200 H 8.10 mg/m3 1.00 1.00 1 08/23/2019 13'02 Digestion for TKN SM 4500 NorgD Complete I 08/14/2019 13:13 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 1 08/08/2019 15:50 ANALYTICAL RESULTS Report 4 0819_MRCO_11 Location: JH_PARK Field ID: AF56194 Lab ID: AF56194 Collect Date/Time: 8/7/19 08:47 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N <MDL t! mg/L 0.011 0.020 I 08/09/2019 12:08 Enterococci EnterolertlQT 10 <130 MPN/100 ml 10 10 10 08/07/2019 14:22 Digestion for Metals EPA 200.8 Completed 7 08/13/2019 09:25 Phosphorus-Total EPA 200.8 .0.066 <0.046 1 mg/L 0.028 0.070 7 08/15/2019 12:31 Nitrogen-Total Kjeldahl EPA 351.2 0.707 mg/L 0.230 0.500 I 08/19/2019 16.07 Nitrate-Nitrite(N) EPA 353.2 0.011 U mg/L 0.011 0.020 I 08/08/2019 14:26 pH FDEP FT 1100 8.0 6.5-8.5 SU 1 08/07/2019 08:47 Dissolved Oxygen Saturation FDEP FT1500 113.6 >42 % I 08/07/2019 08:47 Nitrogen-Total Nitrogen-Total 0.707 <0.3 mg/L 0.230 0.500 1 08/20/2019 09:26 Chlorophyll a SM 10200 H 7.2 <4.9 mg/m3 1.00 1.00 I 08/23/2019 13.02 Filtration for Chlorophyll and Phi SM 10200 H Completed 1 08/07/2019 1431 Pheophytin SM 10200 H 6.70 mg/m3 1.00 1.00 I 08/23/2019 13:02 Digestion for TKN SM 4500 NorgD Complete 1 08/14/2019 13:15 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 1 08/08/2019 15:51 ANALYTICAL RESULTS Report 4 0819_MRCO_II Location: COLLIER_BRIDGE Field ID: AF56195 Lab ID: AF56195 Collect Date/Time: 8/7/19 10:58 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N <MDL U melt 0.011 0.020 1 08/09/2019 12:08 Enterococci Enterolert/QT 63 <130 MPN/100 mL 10 10 10 08/07/2019 1422 Digestion for Metals EPA 200.8 Completed 7 08/13/2019 09:25 Phosphorus-Total EPA 200.8 0.085 <0 046 mg/L 0.028 0.070 7 08/15/2019 12:34 Nitrogen-Total Kjeldahl EPA 351.2 0.492 I mg/L 0 230 0.500 1 08/19/2019 1606 Nitrate-Nitrite(N) EPA 353.2 0.011 U me/L 0.011 0.020 I 08/08/2019 1431 pH FDEP FTI 100 8.0 6.5-8.5 SU 1 08/07/2019 10:58 Dissolved Oxygen Saturation FDEP FTI 500 145.1 >42 % 1 08/07/2019 10:58 Nitrogen-Total Nitrogen-Total 0.492 <0.3 I mg/L 0 230 0.500 1 08/20/2019 09:26 Chlorophyll a SM 10200 H 1.0 <4.9 U mg/m3 1.00 1.00 1 08/23/2019 13.02 Filtration for Chlorophyll and Phe SM 10200 H Completed 1 08/07/2019 14:31 Pheophytin SM 10200 H 11.5 mg/m3 1.00 1.00 1 08/23/2019 13:02 Digestion for TKN SM 4500 NorgD Complete I 08/14/2019 13:15 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 I 08/08/2019 15:54 ANALYTICAL RESULTS Report#0819_MRCO_1l FL State Laborator ID:£45464 EPA Lab Code:FL00919 Page 5 of 8 Location: HC_CENTER Field ID: AF56196 Lab ID: AF56196 Collect Date/Time: 8/7/19 11:35 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N <MDL U mg/L 0.011 0.020 1 08/0912019 12:08 Enterococci Enterolert/QT 10 <130 MPN/I00 mL 10 10 10 08/07/2019 14:22 Digestion for Metals EPA 200.8 Completed 7 08/13/2019 09:25 Phosphorus-Total EPA 200.8 0.065 <0.046 I mg/L 0.028 0.070 7 08/15/2019 12:38 Nitrogen-Total Kjeldahl EPA 351.2 0.397 1 mg/L 0.230 0.500 1 08/19/2019 16:05 Nitrate-Nitrite(N) EPA 353.2 0.011 U mg/L 0.011 0 020 1 08/08/2019 14:36 pH FDEP FTI 100 8.1 6.5-8.5 SU 1 08/07/2019 11:35 Dissolved Oxygen Saturation FDEP FT1 500 163.3 >42 % 1 08/07/2019 11:35 Nitrogen-Total Nitrogen-Total 0.397 <0.3 1 mg/L 0.230 0.500 1 08/20/2019 09:26 Chlorophyll a SM 10200 H 7.5 <4.9 mg/m3 1.00 1.00 1 08/23/2019 13:02 Filtration for Chlorophyll and Phe SM 10200 H Completed I 08107/2019 14:31 Pheophytin SM 10200 H 1.00 U mg/m3 1.00 1.00 I 08/23/2019 13:02 Digestion for TKN SM 4500 NorgD Complete 1 08/14/2019 13:15 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 I 08/08/2019 15:57 ANALYTICAL RESULTS Report 4 0819_MRCO_11 Location: KENDALL Field ID: AF56197 Lab ID: AF56197 Collect Date/Time: 8/7/19 10:27 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N <MDL U ma/L 0.011 0.020 I 08/09/2019 12:08 Enterococci Enterolert/QT 10 <130 U MPN/100 mL 10 10 10 08/07/2019 14:22 Digestion for Metals EPA 200.8 Completed 7 08/13/2019 09:25 Phosphorus-Total EPA 200.8 0.074 <0.046 mg/L 0.028 0.070 7 08/15/2019 12:41 Nitrogen-Total Kjeldahl EPA 351 2 0.590 mg/L 0.230 0.500 I 08/19/2019 16:03 Nitrate-Nitrite(N) EPA 353.2 0.011 U mg/L 0.011 0.020 1 08/08/2019 14:38 pH FDEP FTI 100 7.9 6.5•8.5 SU I 08/07/2019 10:27 Dissolved Oxygen Saturation FDEP FT1500 105.2 >42 % 1 08/07/2019 10:27 Nitrogen-Total Nitrogen-Total 0.590 <0.3 mg/L 0.230 0.500 I 08/20/2019 0926 Chlorophyll a SM 10200 H 11.7 <4.9 mg/m3 1.00 1.00 I 0$2312019 13:02 Filtration for Chlorophyll and Phi: SM 10200 H Completed I 08/07/2019 14:31 Pheophytin SM 10200 H 1.40 mg/m3 1.00 1.00 I 08/23/2019 13:02 Digestion for TKN SM 4500 NorgD Complete I 08/14/2019 13:15 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 1 08/08/2019 15:58 ANALYTICAL RESULTS Report 4 0819_MRC0_11 Location: FCEB_MARCO Field ID: AF56199 Lab ID: AF56199 Collect Date/Time: 8/7119 11:18 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N <MDL U mg/L 0.011 0.020 1 08/09/2019 12:08 Enterococci Enterolert/QT 10 <I30 U MPN/100 mL 10 10 10 08/07/2019 14-22 FL State Laboratory ID:E45464 EPA Lab Code:FL00919 Page 6 of 8 Digestion for Metals EPA 200.8 Completed I 08/13/2019 09:25 Phosphorus-Total EPA 200.8 0 004 <0.046 U mg./L 0.004 0.010 I 08/15/2019 13:13 Nitrogen-Total Kjeldahl EPA 351.2 0 230 U mg/L 0.230 0.500 I 08/19/2019 17:42 Nitrate-Nitrite(N) EPA 353.2 0 011 U mg/L 0.011 0.020 I 08/08/2019 14:41 pH FDEP FTI 100 NA 6.5-8.5 SU I 08/07/2019 11:18 Dissolved Oxygen Saturation FDEP FTI500 NA >42 % 1 08/07/2019 11:18 Nitrogen-Total Nitrogen-Total <MDL't'i <0.3 U mg/L 0.230 0.500 1 08/20/2019 09:26 Chlorophyll a SM 10200 H 1.0 <4.9 U mg'm3 1.00 1.00 I 08/23/2019 13:02 Filtration for Chlorophyll and Phe SM 10200 H Completed I 08/072019 14:31 Phcophytin SM 10200 H 1.00 U mg/m3 1.00 1.00 I 08/23/2019 13:02 Digestion for TKN SM 4500 NorgD Complete 1 08/14/2019 13:15 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 1 08/08/2019 16:01 ANALYTICAL RESULTS Report#0819_MRCO_I Location: EB MARCO Field ID: AF56200 Lab ID: AF56200 Collect Daterrime: 8/7/19 08:40 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N <MDL U mg/L 0.011 0.020 1 08/09/2019 12:08 Enterococci Enterolert/QT 10 13(1 U MPN/100 mt. 10 10 10 08/07/2019 14:22 Digestion for Metals EPA 200.8 Completed 1 08/13/2019 0925 Phosphorus-Total EPA 200.8 0.004 <0-046 U mg/L 0.004 0.010 1 08/15/2019 13:16 Nitrogen-Total Kjeldahl EPA 351.2 0.230 U mg/L 0.230 0.500 1 08/15/2019 12:01 Nitrate-Nitrite(N) EPA 353.2 0.011 U mg/L 0.011 0.020 1 08/08/2019 14:42 pH FDEP FTI 100 NA 6.5-8.5 SU 1 08/07/2019 08:40 Dissolved Oxygen Saturation FDEP FT1500 NA >42 % 1 08/07/2019 08:40 Nitrogen-Total Nitrogen-Total '1,41DL <0.3 U mg/L 0.230 0.500 1 08/15/2019 15:29 Chlorophyll a SM 10200 11 1.0 <4.9 U mg/m3 1.00 1.00 1 08232019 13:02 Filtration for Chlorophyll and Phe SM 10200 H Completed 1 08/08/2019 11:30 Pheophytin SM 10200 H 1.00 U mg/m3 1.00 1.00 I 08/23/2019 13:02 Digestion for TKN SM 4500 NorgD Complete I 08/13/2019 09:54 Nitrite(N) SM 4500-NO2 B 0.002 1'' mg/L 0.002 0.005 I 08/08/2019 16:02 ANALYTICAL RESULTS Report#0819_MRC0_I Location: DUP1 Field ID: AF56201 Lab ID: AF56201 Collect Date?rme: 8/7119 09:24 Acceptable Analyte Name Method Result Limits Qualifier Units MDL PQL DF Analysis Date/Time CC-Nitrate-N CC-Nitrate-N 0.013 1 mg/L 0.011 0.020 1 08/092019 12:08 Enterococci Enterolert/QT 10 <130 U MPN/100 mL 10 10 10 08/07/2019 14:22 Digestion for Metals EPA 200.8 Completed 7 08/132019 09:25 Phosphorus-Total EPA 200.8 0.071 <0.046 mg/L 0.028 0.070 7 08/15/2019 12:57 Nitrogen-Total Kjeldahl EPA 351.2 0.543 inv./1_ 0.230 0.500 1 08/15/2019 11:58 Nitrate-Nitrite(N) EPA 353.2 0.013 1 mg/L 0.011 0.020 1 08/08/2019 14:43 FL State Laboratory ID:E.45464 EPA Lab Code:FL00919 Page 7 of 8 pH FDEP FT1100 7.7 6.5-8.5 SU I 08/07/2019 09:24 Dissolved Oxygen Saturation FDEP FT1500 75 8 >42 % 1 08/07/2019 09:24 Nitrogen-Total Nitrogen-Total 0.556 <0.3 mg;L 0.230 0.500 I 08/15/2019 15:29 Chlorophyll a SM 10200 H 3 4 <4.9 J mg/m3 1.00 1.00 1 08/232019 13:02 Filtration for Chlorophyll and Phe SM 10200 H Completed I 08/082019 11:30 Pheophytin SM 10200 H 6.80 J mgim3 1.00 1.00 I 08232019 13.02 Digestion for TKN SM 4500 NorgD Complete 1 08/13/2019 09:54 Nitrite(N) SM 4500-NO2 B 0.002 U mg/L 0.002 0.005 1 08/082019 16:03 Fl.Stale Laboratory ID:E45464 EPA Lab Code:FL00919 Page 8 of 8